In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 75476-78-7 as follows. SDS of cas: 75476-78-7
Next, 30% H2O21.5L and 300 ml of formic acid is added during the reaction of the bottle, which is controlled from a temperature of 35 C prepd. 40 C in b Furthermore, with the added 148g of compound 8. The reaction mixture is stirred at room temperature for 12 hours. After that, a large amount of water is poured on the reaction, the precipitated solid white, which is filtered. Furthermore, the third port 3L 5L of 7% aqueous sulfuric acid is added to the flask, then heated up to boiling. The white solid reaction is added to the bottle, attached to the distillation, 64g compd. 9 (white solid state) is obtained. The reaction of the pathway of the following relationships
According to the analysis of related databases, 75476-78-7, the application of this compound in the production field has become more and more popular.
Reference:
Patent; DAXIN MATERIALS CORPORATION; LEE, CHING-TIEN; LIU, HSIN-CHENG; WANG, CHUN-CHIH; JIANG, TIAN-MENG; TIAN, HUI-QUIANG; GAO, LI-LONG; HUANG, WAN-YU; (47 pag.)JP2016/29040; (2016); A;,
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