Continuously updated synthesis method about 2550-36-9

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2550-36-9.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2550-36-9, name is (Bromomethyl)cyclohexane, This compound has unique chemical properties. The synthetic route is as follows., Formula: C7H13Br

2,6-dihydroxy acetophenone solution (2,6-dihydroxyacetophenone, compound 7, 1.0 eq.), Anhydrous potassium carbonate (anhydrouspotassium carbonate, 2.0 eq.), Dissolved in acetone, alkyl bromide mixture (alkyl bromides, 1.0 eq.) Were mixed and it reacted for 18 hours at 70 ~ 80 . After evaporation of acetone, the remaining reaction product was diluted with dichloromethane and washed three times in water. The organic layer was then collected and concentrated under reduced pressure and then dehydrated with anhydrous Na2SO4 and the crude product obtained by separating the crude product was purified by column chromatography to obtain a compound 9a ~ 9d.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2550-36-9.

Reference:
Patent; Chungnam National University Industry-Academic Cooperation Foundation; Chungbuk National University Industry-Academic Cooperation Foundation; Jung, Sang Hun; Kim, Young Soo; (39 pag.)KR101535119; (2015); B1;,
Bromide – Wikipedia,
bromide – Wiktionary