Some tips on 556-96-7

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 556-96-7.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 556-96-7, name is 1-Bromo-3,5-dimethylbenzene, This compound has unique chemical properties. The synthetic route is as follows., Product Details of 556-96-7

General procedure: In an oven dried round bottomed flask a mixture containing styrene (2.5mmol), aryl halide (2.5mmol), the palladium complex [Pd(OL1)]4 (0.005mmol) and potassium carbonate (10.0mmol) in methanol (10cm3) was heated to reflux for 4h, as mentioned in Table 3. After the reaction was completed, the solvent was evaporated and the reaction mixture was extracted with diethyl ether. The ether solution was dried over Na2SO4 and filtered. The ether solution, containing the reaction mixture, was passed through a 12.48cm silica column (60-120 mesh), the complex was not separated out and it remained trapped in the column. After he desired compound was extracted from the column, the complex was eluted using dichloromethane. Upon evaporation of the ether, solids of the pure products were obtained. The yields of the products obtained from all the reactions were determined after isolation, and the products were characterized by 1H NMR spectra.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 556-96-7.

Reference:
Article; Pattanayak, Poulami; Pratihar, Jahar Lal; Patra, Debprasad; Lin, Chia-Her; Chattopadhyay, Surajit; Polyhedron; vol. 63; (2013); p. 133 – 138;,
Bromide – Wikipedia,
bromide – Wiktionary