Adding a certain compound to certain chemical reactions, such as: 1073-06-9, name is 1-Bromo-3-fluorobenzene, belongs to bromides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1073-06-9, HPLC of Formula: C6H4BrF
General procedure: In a typical run, a 5-mL vial equipped with a magnetic stirrer was charged with a mixture of phenyl bromide(78.5 mg, 0.5 mmol), styrene (62.5 mg, 0.6 mmol), Pd catalyst (0.0025 mmol), K3PO4 (212 mg, 1.0 mmol) and DMF (1 mL) under nitrogen. The mixture was heated at 100 C for 4 h and then cooled to room temperature. Brine was added, and the resulting mixture was extracted with ethyl acetate (3 x 5 mL). The GC-MS samples were prepared by diluting 10 lL of ethyl acetate solution to1 mL.
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Reference:
Article; Du, Yufeng; Liang, Beibei; Yang, Fenglei; Shi, Yanhui; Li, Xiuling; Pang, Guangsheng; Cao, Changsheng; Transition Metal Chemistry; vol. 42; 3; (2017); p. 193 – 201;,
Bromide – Wikipedia,
bromide – Wiktionary