In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,4-Dibromo-2,5-dihexylbenzene, other downstream synthetic routes, hurry up and to see.
Electric Literature of 117635-21-9, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 117635-21-9, name is 1,4-Dibromo-2,5-dihexylbenzene belongs to bromides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
In the reaction vessel, 1,4-dibromo-2,5-dihexylbenzene (0.81 g, 2.0 0 mmol),20 ml of tetrahydrofuran was added, and at -78 C.,The mixture was stirred. Thereafter, 1.6 M n-butyllithium (n-BuLi) hexane solution (2.53 ml, 4.00 mmol) was added dropwise and after stirring for 1 hour, 3,5-diphenyl- 1-chlorotriazine was added , And the mixture was stirred at room temperature for 3 hours.After completion of the reaction, water was added to the reaction mixture,The mixture was extracted with chloroform, and the organic layer was concentrated. after that,Tetrahydrofuran was added to and dissolved in the resulting residue,Purification was carried out by reprecipitation twice using methanol to obtain a compound B.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,4-Dibromo-2,5-dihexylbenzene, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; SAMSUNG ELECTRONICS COMPANY LIMITED; SHIBATA, KATSUNORI; ISHII, HIROTO; MOTOYAMA, TAKAO; (23 pag.)JP2016/108255; (2016); A;,
Bromide – Wikipedia,
bromide – Wiktionary