Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 10016-52-1, name is 2,8-Dibromodibenzo[b,d]furan, This compound has unique chemical properties. The synthetic route is as follows., 10016-52-1
30.0 g (92.03 mmol) of 2,8-dibromodibenzo [b, d] furan, 25.1 g (184.06 mmol) of 1- (3-hydroxyphenyl) ethanone in a 500 mL reactor,1.8 g (9.20 mmol) of iodo copper,1,10-phenanthroline 3.3 g (18.41 mmol),Add 38.2 g (276.09 mmol) of anhydrous potassium carbonate, add 400 ml of N, N-dimethylformamide and stir at reflux for 24 hours under a nitrogen atmosphere.After completion of the reaction, extracted with ethyl acetate, distilled water,Filtered by anhydrous magnesium sulfate,Purified by silica gel chromatography, 20.9 g (52% yield) of an intermediate compound [2-1] as an off-white solid were prepared
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Reference:
Patent; Teuri L Co., Ltd.; Kang Ji-seung; Moon Bong-seok; Jin Seong-min; Hong Won-gi; Ha Min-su; Lee Gyu-seong; Jin Sang-jun; Park No-gil; Lee Hyeon-u; Byun U-geun; (50 pag.)KR2019/139404; (2019); A;,
Bromide – Wikipedia,
bromide – Wiktionary