89359-54-6, A common compound: 89359-54-6, name is 9-Bromo-1-nonene, belongs to bromides-buliding-blocks compound, it can change the direction of chemical reaction, and react with certain compounds to generate new functional products. A new synthetic method of this compound is introduced below.
Synthesis of compound 19 ?CF2CF3 ^CF2CF3 19 A 5 ml flask was charged with alkene 6 (0.5 g, 2.44 mmol), thiol CF3CF2(CH2)3SH (0.47 g, 2.44 mmol), 2,2-dimethoxy-2-phenyl-acetophenone (12 mg, 0.05 mmol) and CHCI3 (1 .5 ml) and purged with nitrogen atmosphere. The mixture was stirred at room temperature and irradiated with UV black light for 3 h (lambda = 365-368 nm, 15W). The mixture was concentrated by evaporating the solvent. An oil was obtained (0.96 g, 192%).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 9-Bromo-1-nonene, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; CRYSTAL PHARMA, S.A.U.; PEREZ ENCABO, Alfonso; TURIEL HERNANDEZ, Jose Angel; GALLO NIETO, Francisco Javier; LORENTE BONDE-LARSEN, Antonio; GARCIA ESCUDERO, Luis Angel; WO2015/181116; (2015); A1;,
Bromide – Wikipedia,
bromide – Wiktionary