Adding a certain compound to certain chemical reactions, such as: 7766-50-9, name is 11-Bromo-1-undecene, belongs to bromides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 7766-50-9, Recommanded Product: 7766-50-9
To a solution of 11-Bromoundec-1-ene (2.2 mL, 10.1 mmol) in dry DMF (100 mL) was added 0.75 g (10.1 mmol) of NaN3. The solution was stirred for 12 h at room temperature. The reaction mixture was poured into 20 mL water and extracted with ethyl acetate (2 x 30 mL). The combined organic layer was washed with saturated NaCl solution and dried over anhydrous Na2SO4. Solvent was removed under reduced pressure to obtain the product as yellow oil. The product was used for the next step without any further purification. Yield: 1.9 g (96 %).Rf: 0.96 (1:9 Ethyl acetate & Cyclohexane).1H-NMR (CDCl3, 300 MHz, ppm): delta = 1.30 (s, 12H), 1.60 (m, 2H), 2.05 (m, 2H), 3.26 (t, J = 7.0 Hz, 2H), 4.96 (m, 2H), 5.83 (m, 1H). 13C-NMR (CDCl3, 75 MHz, ppm): delta = 26.9, 29.0, 29.1, 29.3, 29.3, 29.5, 29.6, 34.0, 51.7, 114.3, 139.3.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 11-Bromo-1-undecene, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Bhabak, Krishna P.; Proksch, Denny; Redmer, Susanne; Arenz, Christoph; Bioorganic and Medicinal Chemistry; vol. 20; 20; (2012); p. 6154 – 6161;,
Bromide – Wikipedia,
bromide – Wiktionary