89359-54-6, name is 9-Bromo-1-nonene, belongs to bromides-buliding-blocks compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. Recommanded Product: 89359-54-6
REFERENCE EXAMPLE 14 Methyl 2-methyl-2-(8-nonenyloxy)propionate To 500 ml of dry N,N-dimethylformamide, 17 g of 60% sodium hydride was added, and 48 g of methyl 2-hydroxyisobutyrate was added dropwise with stirring under ice-cooling, and stirred for 10 minutes. Then, 100 g of 9-bromo-1-nonene (purity: 63.4%) was added, and the mixture was stirred for 15 hours at room temperature. The reaction solution was poured into ice-cold water, extracted with ethyl acetate, washed with brine, dried over anhydrous magnesium sulfate and concentrated. The residue was distilled under reduced pressure to give 29.9 g of the objective compound as yellowish oil. B.p. 124-127 C. (8 mmHg).
The synthetic route of 89359-54-6 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Kuwabara, Kenji; Aoki, Tomiyoshi; US2003/166697; (2003); A1;,
Bromide – Wikipedia,
bromide – Wiktionary