Related Products of 4117-09-3,Some common heterocyclic compound, 4117-09-3, name is 7-Bromo-1-heptene, molecular formula is C7H13Br, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
In a round-bottom flask, tetrabutylammonium iodide(0.02 eq.) and potassium phthalimide (2.0 eq.) were suspended in acetonitrile. 17 (1.0 eq.) was addeddropwise and the resulting mixture was heated up to 80C for exactly 24 hours. Once the mixturereached room temperature, it was diluted with diethyl ether and passed through a celite plug. Thefiltrate was concentrated in vacuo and the yellow residue was purified by column chromatography(hexane/ethyl acetate 95/5) giving the desired product as a white solid (83% yield).
The synthetic route of 4117-09-3 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Czescik, Joanna; Zamolo, Susanna; Darbre, Tamis; Mancin, Fabrizio; Scrimin, Paolo; Molecules; vol. 24; 15; (2019);,
Bromide – Wikipedia,
bromide – Wiktionary