Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2576-47-8, name is 2-Bromoethylamine hydrobromide, This compound has unique chemical properties. The synthetic route is as follows., SDS of cas: 2576-47-8
Reference Example 66Benzyl 2-bromoethylcarbamate To a solution prepared by adding 1,4-dioxane (50 mL) to benzyl chloroformate (17.5729 g; manufactured by Wako Pure Chemical Industries, Ltd.), an aqueous solution of 2-bromoethanamine hydrobromide-1,4-dioxane [104 mL; solution prepared by dissolving 2-bromoethanamine hydrobromide (21.3617 g; manufactured by Tokyo Chemical Industry Co., Ltd.) in water (54 mL) and 1,4-dioxane (54 mL)]and a 2 mol/L aqueous solution of sodium hydroxide (104 mL; manufactured by Kanto Chemical Co., Inc.) were simultaneously added dropwise. The mixture was stirred for 2 hours at 0 C. Water was added to the reaction solution, and the mixture was extracted two times with ethyl acetate. The organic layer was washed with a saturated solution of sodium hydrogen carbonate, and was dried over magnesium sulfate. The organic layer was concentrated under reduced pressure. The resulting residue was purified by column chromatography (?COLUMN-A?; n-hexane:ethyl acetate=94:6?73:27), and thus the title compound (19.2014 g) was obtained.1H-NMR (300 MHz, CDCl3); delta(ppm) 3.47(2H, t, J=5.8), 3.60(2H, t, J=5.8), 5.11(2H, s), 7.27-7.40(5H, m)LCMS: 258 [M+H]; Retention time: 1.42 minutes; LCMS condition; C
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2576-47-8.
Reference:
Patent; ASAHI KASEI PHARMA CORPORATION; US2010/160256; (2010); A1;,
Bromide – Wikipedia,
bromide – Wiktionary