Reference of 556-96-7, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 556-96-7 as follows.
General procedure: Styrene (5.0 mmol), aryl halide (5.0 mmol), potassium carbonate(10.0 mmol) and the palladium complex (0.003 mmol) weremixed in methanol (20 ml) and refluxed for 2 h as mentioned inTable 5. At the end of the reaction solvent was evaporated andthe residue was poured into water and extracted in diethyl ether,dried over anhydrous Na2SO4 and pass through 12// silica column (60-120 mesh). After evaporation of the ether, solid pure productswere obtained. The yields of the products obtained from all thereactions were determined after isolation and characterized by1H NMR spectra (Table 5).
According to the analysis of related databases, 556-96-7, the application of this compound in the production field has become more and more popular.
Reference:
Article; Das, Uttam; Pattanayak, Poulami; Patra, Debprasad; Brandao, Paula; Felix, Vitor; Chattopadhyay, Surajit; Polyhedron; vol. 110; (2016); p. 165 – 171;,
Bromide – Wikipedia,
bromide – Wiktionary