A new synthetic route of 1,2-Dibromo-3,4,5,6-tetrafluorobenzene

According to the analysis of related databases, 827-08-7, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 827-08-7, name is 1,2-Dibromo-3,4,5,6-tetrafluorobenzene, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C6Br2F4

EXAMPLE 1 1,4-bis(dipentafluorophenylboryl)-2,3,5,6-tetrafluorobenzene 1.54 g (5 mmol) of dibromotetrafluorobenzene are dissolved in 40 ml of n-hexane and cooled to -78 C. 6.4 ml of n-BuLi (10 mmol) are slowly added dropwise to the solution and the mixture is stirred for 1 hour. Subsequently, 1.90 g (5 mmol) of bis(pentafluorophenyl)borylchloride are dissolved in 40 ml of n-hexane and likewise added dropwise to the above solution. The suspension obtained is slowly warmed to room temperature, forming a white precipitant. This is separated off by filtration and the filtrate obtained is evaporated to dryness under reduced pressure. The yield of the resulting 1,4-bis(dipentafluorophenylboryl)-2,3,5,6-tetrafluorobenzene obtained as a yellow oil is 81%.

According to the analysis of related databases, 827-08-7, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Targor GmbH; US6255531; (2001); B1;,
Bromide – Wikipedia,
bromide – Wiktionary