Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 960203-41-2, name is (2-Bromophenyl)(2,4-dimethylphenyl)sulfane, This compound has unique chemical properties. The synthetic route is as follows., Application In Synthesis of (2-Bromophenyl)(2,4-dimethylphenyl)sulfane
Intermediate 1 (Formula IV) obtained in the manner of Example 1 (10.0 g, 34 mmol),N-Boc-piperazine (7.0 g, 38 mmol) was dissolved in 50 ml of toluene.The mixture was stirred under nitrogen for 10 minutes at room temperature (25 C). To the mixture was added tris(dibenzylideneacetone)dipalladium (312 mg, 0.34 mmol),Racemic 2,2-bis(diphenylphosphino)-1,1-biphenyl (637 mg, 1.02 mmol),Sodium tert-butoxide (3.9 g, 41 mmmol),Re-nitrogen replacement.Heat to reflux under nitrogen and react for 12 h.After the reaction was completed, it was cooled to room temperature and filtered through celite.The filtrate was washed with saturated brine and toluene was removed under reduced pressure.Obtained a brown oil(N-Boc-fluoxetine) 14.2 g.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 960203-41-2.
Reference:
Patent; Shandong Jingwei Pharmaceutical Co., Ltd.; Guo Xiao; Liu Qun; Sang Wei; Qu Aicun; Sun Huifeng; (13 pag.)CN110054600; (2019); A;,
Bromide – Wikipedia,
bromide – Wiktionary