Reference of 2576-47-8,Some common heterocyclic compound, 2576-47-8, name is 2-Bromoethylamine hydrobromide, molecular formula is C2H7Br2N, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
2-Bromoethylamine hydrobromide (500 mg, 2.44 mmol) and sodium azide (475.9 mg, 7.32 mmol) were dissolved in water (2 mL). The solution was heated to 75 C, stirred for 21 h, cooled to 0 C, Potassium (800 mg) and diethyl ether (2 mL). Purified by chloroform-methanol (20:1) column chromatography2-azidoethylamine (171 mg, 82%).
The synthetic route of 2576-47-8 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; China Institute Of Forestry Forest Products Chemical Industry Institute; Nanjing Zhongsen Biological Technology Co., Ltd.; Wang Chengzhang; Qi Zhiwen; (7 pag.)CN109180594; (2019); A;,
Bromide – Wikipedia,
bromide – Wiktionary