Share a compound : C6H11Br

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 6-Bromo-1-hexene, and friends who are interested can also refer to it.

Adding a certain compound to certain chemical reactions, such as: 2695-47-8, name is 6-Bromo-1-hexene, belongs to bromides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 2695-47-8, SDS of cas: 2695-47-8

Sodium hydride (1.05 eq) was slowly added at 00C to a solution of iV-methyltrifluoro- acetamide (25 g) in DMF (140 mL). The mixture was stirred for Ih at room temperature under nitrogen. Then, a solution of bromohexene (32.1 g) in DMF (25 niL) was added dropwise and the mixture was heated to 70C for 12 hours. The reaction mixture was poured on water (200 mL) and extracted with diethylether (4 x 50 mL), dried (MgSO4), filtered and evaporated to give 35 g of the target product (1-5) as a yellowish oil which was used without further purification in the next step.

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 6-Bromo-1-hexene, and friends who are interested can also refer to it.

Reference:
Patent; Tibotec Pharmaceuticals Ltd.; WO2008/59046; (2008); A1;,
Bromide – Wikipedia,
bromide – Wiktionary