Reference of 3344-70-5, These common heterocyclic compound, 3344-70-5, name is 1,12-Dibromododecane, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Phenothiazine and 1,12-dibromododecane (molar ratio = 1:10), potassium hydroxide and DMSO were added to a three-necked flask, filledwith nitrogen, and stirred at room temperature for 12 hours. The reaction mixture was washed with water and extracted with dichloromethane. , Drying over anhydrous, vortexing, andsilica gel column chromatographywith petroleum ether aseluent to give a colorless liquid in a yield of 76.5percent.
Statistics shows that 1,12-Dibromododecane is playing an increasingly important role. we look forward to future research findings about 3344-70-5.
Reference:
Patent; Jiangxi Agricultural University; Hong Yanping; Jiang Yan; Yin Xiaoli; Wu Guoqiang; Liao Xiaoning; Wang Chunrong; Li Liyu; (27 pag.)CN107698999; (2018); A;,
Bromide – Wikipedia,
bromide – Wiktionary