Electric Literature of 60956-23-2, A common heterocyclic compound, 60956-23-2, name is 1,2-Dibromo-4-methylbenzene, molecular formula is C7H6Br2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Add 4-methyl-o-dibromobenzene (1.0 mmol), tBuOOH (1.5 mmol), andCu (acac) 2 (0.06mmol), then add 2mL of solvent water, and react at room temperature for 10 hours,After the reaction was completed, the reaction solution was concentrated, and the corresponding product was obtained by column chromatography. The isolated yield was 93%.
The synthetic route of 60956-23-2 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Shanghai Institute of Technology; Yao Zijian; Qiao Xinchao; (6 pag.)CN110981702; (2020); A;,
Bromide – Wikipedia,
bromide – Wiktionary