Adding a certain compound to certain chemical reactions, such as: 1074-24-4, name is 1,4-Dibromo-2,5-dimethylbenzene, belongs to bromides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1074-24-4, COA of Formula: C8H8Br2
1,4-dibromo-2,5-dimethylbenzene: 1H-1,2,4-triazole: potassium carbonate: copper oxide molar ratio is 2: 10: 30: 1. A 50mL three-neck round bottom flask equipped with a magnetic stirrer, reflux condenser and thermometer was added CuO (0.0398mg,0.5mmol), potassium carbonate (2.0731g, 15mmol), 1H-1,2,4-triazole (0.345mg, 5mmol), 1,4- dibromo-2,5-dimethylbenzene (0.3360g, 1mmol ), 20mL DMAC. Start stirring at 100 deg.C and react for 24 hours. After completion of the reaction, the reaction solution was cooled to room temperature, filtered and the filtrate was added 100mL of water, heavy precipitate precipitation, filtration, filter cake was collected, yield 60percent.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,4-Dibromo-2,5-dimethylbenzene, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Tianjin Normal University; Wang, Zhongliang; Wang, Ying; (12 pag.)CN105732719; (2016); A;,
Bromide – Wikipedia,
bromide – Wiktionary