Reference of 7314-86-5,Some common heterocyclic compound, 7314-86-5, name is 1,3,5,7-Tetrabromoadamantane, molecular formula is C10H12Br4, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Compound (1) of Example Ia was reacted with sodium cyanide in DMSO under irradiation at 254 nm as described in G. S. Lee et al., Org. Lett. Vol. 6, No. 11, 2004, 1705-1707, scheme 2a, (c). Tetracyanoadamantane was obtained in 63% yield.
The synthetic route of 7314-86-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; GE HEALTHCARE AS; WO2009/21948; (2009); A1;,
Bromide – Wikipedia,
bromide – Wiktionary