Related Products of 105309-59-9, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 105309-59-9, name is Tetrakis(4-bromophenyl)methane belongs to bromides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
A 250 mE Schlenk flask was charged with A (4 g,6.3 mmol), 13 (6.79 g, 37.7 mmol), CsF (9.5 g, 63.9 mmol),and Pd(P(Ph)3)4 0.3 g. 120 ml DME was degassed and transferred. A water condenser was then equipped. The flask washeated to reflux under the nitrogen for 48 hours. The solventwas dried on rotary evaporator. The residue was dissolved byCH2C12, and purified by column chromatography to get C 4.1g (Yield. 76%).
The synthetic route of Tetrakis(4-bromophenyl)methane has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Zhou, Hong-Cai; Feng, Dawei; Wang, Kecheng; US2015/152123; (2015); A1;,
Bromide – Wikipedia,
bromide – Wiktionary