Related Products of 89523-51-3, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 89523-51-3 as follows.
Argon atmosphere, 3-bromo-fluoranthene 12.3g, 2-chloroaniline 5.60g, tris-dibenzylideneacetone dipalladium (0) 0.732g, Tri-t-butylphosphine tetrafluoroborate dihydro 0.926g borate, -t- sodium butoxide, 7.68g, was stirred in a 400mL flask, and dehydrated toluene, heated at 80 8 hours. After cooling to room temperature (25 ), the reaction solution was extracted with toluene, and was filtered through Celite. Filtrate was concentrated, and the residue was purified by column chromatography on silica gel, 5- (2-chloro-2,3,4) benzo [c] phenanthrene was obtained a 11.32g.
According to the analysis of related databases, 89523-51-3, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Idemitsu Kosan Corporation; Kawamura, Masahiro; Mizuki, Yumiko; Ito, Hirokazu; Hayama, Tomoharu; Haketa, Tasuku; (69 pag.)KR2015/126340; (2015); A;,
Bromide – Wikipedia,
bromide – Wiktionary