Related Products of 629-03-8, The chemical industry reduces the impact on the environment during synthesis 629-03-8, name is 1,6-Dibromohexane, I believe this compound will play a more active role in future production and life.
Preparation of 6-Bromohex-1-ene 1,6-Dibromohexane (30 mL, 48 g) was placed in a PTFE reactor vessel along with a magnetic stirrer bar. The reactor was set up with a 3 mm O.D. outlet tube connected to the cover assembly. The dibromide was heated to 150 C. and hexamethylphosphorous triamide (HMPTA; ca. 3 mL) was added through a second tube attached to the cover assembly, by means of a syringe. The vessel contents were then heated to 200 C. and HMPTA (42 mL) was added dropwise through the syringe. The crude product distilled through the exit tube and was collected in chilled flasks, then redistilled to give 6-bromohex-1-ene (15.6 g, 49%). 1 H NMR (CDCl3; 200 MHz): delta1.56, m, 2H, CH2; 1.85, m, 2H, CH2; 2.10, m, 2H, CH2; 3.41, t, J=7 Hz, 2H, CH2 Br; 4.85-5.10, m, 2H, =CH2; 5.80, m, 1H, =CH, in agreement with that reported by Kenneth J.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,6-Dibromohexane, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Commonwealth Scientific and Industrial Research Organisation; US5932075; (1999); A;,
Bromide – Wikipedia,
bromide – Wiktionary