Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 24358-62-1, name is 1-(4-Bromophenyl)ethylamine, A new synthetic method of this compound is introduced below., Quality Control of 1-(4-Bromophenyl)ethylamine
General procedure: Into a screw cap reaction vial were added a mixture of dry toluene (1.0 mL), immobilized CaLB enzyme (15.0 mg, CaLB-CV-T2-150), the corresponding racemic amine rac-1a-d (0.778 mmol) and the corresponding isopropyl 2-alkoxyacetate 2A-D (1.0 equiv., 0.778 mmol). The reaction mixture was shaken (750 rpm) at 30 C and monitored by taking samples (20 mL) after different reaction times (0.25, 0.5, 1, 2, 3, 4, 6, 8 h). After 8 h, the reactions were worked up.
The synthetic route of 24358-62-1 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Olah, Mark; Kovacs, Daniel; Katona, Gabriel; Hornyanszky, Gabor; Poppe, Laszlo; Tetrahedron; vol. 74; 27; (2018); p. 3663 – 3670;,
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