Some scientific research about 393-36-2

According to the analysis of related databases, 393-36-2, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 393-36-2, name is 4-Bromo-3-(trifluoromethyl)aniline, This compound has unique chemical properties. The synthetic route is as follows., Application In Synthesis of 4-Bromo-3-(trifluoromethyl)aniline

Step 3.1: 3′-Chloro-2-trifluoromethyl-biphenyl-4-amine; A mixture of 5-amino-2-bromobenzotrifluoride (Dakwood Products, Inc.) (500 mg, 2.1 mMol), 3-chlorophenylboronic acid (970 mg, 6.2 mMol, 3 equiv) (Aldrich), Pd(PPh3J4 (70 mg, 0.018 mMol, 0.03 equiv), Na2CO3 (2 M solution in H2O, 5 mL, 10 mMol, 4.76 equiv), and toluene (14 mL) is stirred at reflux for 1 h. The reaction mixture is allowed to cool to rt and filtered through a pad of celite, washing the filter cake with CH2CI2 and H2O. The layers are EPO separated and the aqueous phase is extracted with CH2CI2 (2 x 60 ml_). The combined organic phase is washed with brine, dried (Na2SO4), filtered and concentrated in vacuo. MPLC (CH3CNZH2OrTFA) purification of the crude material affords the title compound: MS: 270.0 [M-2]”; HPLC DtRef = 4.9.

According to the analysis of related databases, 393-36-2, the application of this compound in the production field has become more and more popular.

Reference:
Patent; NOVARTIS AG; NOVARTIS PHARMA GMBH; WO2006/108640; (2006); A1;,
Bromide – Wikipedia,
bromide – Wiktionary