Synthetic Route of 4101-68-2, The chemical industry reduces the impact on the environment during synthesis 4101-68-2, name is 1,10-Dibromodecan, I believe this compound will play a more active role in future production and life.
General procedure: The bromide or iodide salts of 1,n-bis(isoquinolinium)alkane dications (n = 2, 4, 5, 6, 8, 9, 10 and 12) and alpha,alpha’-bis(isoquinolinium)-p-xylene dibromide were prepared using modifications of a method outlined by Kuca et al.. A mixture of the appropriate 1,n-bis(isoquinolinium)alkane dibromide or diiodide (1.0 mmol) or alpha,alpha’-dibromo-p-xylene (1.0 mmol) and isoquinoline (9.0 mmol) in DMF was heated at 70 C for 1-4 days. The addition of diethyl ether to the cooled solution resulted in a light brown precipitate, which was filtered and washed with diethyl ether.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,10-Dibromodecan, other downstream synthetic routes, hurry up and to see.
Reference:
Conference Paper; Kwok, Julian C.; Macartney, Donal H.; Supramolecular Chemistry; vol. 26; 3-4; (2014); p. 182 – 191;,
Bromide – Wikipedia,
bromide – Wiktionary