Related Products of 15155-41-6, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 15155-41-6 as follows.
Synthesis of 3,6-dibromobenzene-1,2-diamine: Dibromobenzo[c][1,2,5]thiadiazole (2.29 g, 10 mmol) and sodiumborohydride (5.7 g, 150 mmol) were added to ethanol at 0 Cand stirred at room temperature for 36 h. The solution wasadded water and ethyl acetate then was separated by separatoryfunnel. The organic layer was dried over MgSO4 then concentrated under reduced pressure and purified by chromatographyon a silica column eluting with petroleum ether/ethyl acetate(5:1, v/v) to afford a yellow solid (1.9 g, 71 % yield). 1H NMR(400 MHz, CDCl3, ppm) delta-aromatic H, 6.86 (d, 2H), 3.92 (s,4H); 13C NMR (100 MHz, CDCl3, ppm): 133.73,123.27, 109.70.
According to the analysis of related databases, 15155-41-6, the application of this compound in the production field has become more and more popular.
Reference:
Article; Sun, Xiaoxia; Lei, Xiaolong; Hu, Yu; Asian Journal of Chemistry; vol. 27; 7; (2015); p. 2427 – 2430;,
Bromide – Wikipedia,
bromide – Wiktionary