Reference of 61613-22-7, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 61613-22-7, name is 2-Bromo-N-phenylaniline belongs to bromides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
To a vacuum dried 250 ml three-neck round bottom flask was added compound 9-1 (16 g),Anhydrous tetrahydrofuran (120 ml) was added and stirred under argon atmosphereThe temperature of the mixture was lowered to -78.Butyllithium (56.75 ml) was added slowly and stirred at the same temperature for 1 hour.Xanthone (15.18 g) was added at the same temperature and stirred for 12 hours.After concentration under reduced pressure, the residue was extracted with chloroform (320 ml) to obtain 8 g of the title compound.
The synthetic route of 2-Bromo-N-phenylaniline has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Dae Joo Electronic Materials Co., Ltd.; Park Jeong-gyu; Jang Sun-uk; Lee Hyeon-seok; Kim Min-yeong; Jeon Yeong-min; (29 pag.)KR2017/126059; (2017); A;,
Bromide – Wikipedia,
bromide – Wiktionary