Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 2606-51-1, name is 5-(Bromomethyl)benzo[d][1,3]dioxole, A new synthetic method of this compound is introduced below., Quality Control of 5-(Bromomethyl)benzo[d][1,3]dioxole
General procedure: Isatin (1 mmol), corresponding benzyl bromide (1 mmol) andK2CO3 (3 mmol) were heated in acetonitrile for 1e2 h. Aftercompletion of the reaction, acetonitrile was removed on rotavoparand the product was extracted using ethyl acetate. The organic layer was dried over anhydrous Na2SO4 and concentrated. Theproduct obtained was used for next step without furtherpurification
The synthetic route of 2606-51-1 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Kamal, Ahmed; Mahesh, Rasala; Nayak, V. Lakshma; Babu, Korrapati Suresh; Kumar, G. Bharath; Shaik, Anver Basha; Kapure, Jeevak Sopanrao; Alarifi, Abdullah; European Journal of Medicinal Chemistry; vol. 108; (2016); p. 476 – 485;,
Bromide – Wikipedia,
bromide – Wiktionary