Analyzing the synthesis route of 7073-94-1

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 7073-94-1.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 7073-94-1, name is 1-Bromo-2-isopropylbenzene, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 7073-94-1

7 g of 2,4,6-trimethylaniline, 10 g of 2-chlorotoluene, 11 g of sodium t-butoxide, 75 mL of toluene was added to the flask, And the mixture was thoroughly stirred under a nitrogen stream. here, Palladium acetate 24 mg, 85 mg of 1,3-bis (2,6-diisopropylphenyl) imidazolium chloride was added, The reaction solution was raised to 110 C., And the mixture was stirred for 3 hours. The obtained reaction solution was cooled and poured into water, And extracted with ethyl acetate. The obtained organic phase was dried over sodium sulfate, After concentration, purification by silica gel column chromatography (developing solution: ethyl acetate / hexane = 1/20) gave 10 g of intermediate 403A.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 7073-94-1.

Reference:
Patent; FUJIFILM CORPORATION; YAGI, KAZUNARI; TATEISHI, KEIICHI; (89 pag.)JP2017/66208; (2017); A;,
Bromide – Wikipedia,
bromide – Wiktionary