Related Products of 615-54-3, These common heterocyclic compound, 615-54-3, name is 1,2,4-Tribromobenzene, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
(2) Synthesis of 2-bromo-N1,N1,N4,N4-tetraphenylbenzene-1,4-diamine 14.74 g of a product (yield: 60%) was obtained in the same manner as described in the synthesis method of intermediate 2-1 except that 1,2,5-tribromobenzene (15.74 g, 50 mmol), diphenylamine (16.92 g, 100 mmol), Pd2(dba)3 (2.75 g, 3 mmol), PPh3 (2.62 g, 10 mmol), NaOt-Bu (28.83 g, 300 mmol), and toluene (525 mL) were used.
The synthetic route of 615-54-3 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; DUKSAN HIGH METAL CO., LTD.; US2012/217492; (2012); A1;,
Bromide – Wikipedia,
bromide – Wiktionary