Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 4101-68-2, name is 1,10-Dibromodecan, A new synthetic method of this compound is introduced below., Recommanded Product: 4101-68-2
Under nitrogen atmosphere, 1.23 g of compound 3, 2.97 g of 1,10-dibromodecane, 0.43 g of potassium hydroxide and 0.16 g Tetrabutylammonium bromide was added to a mixture of 10 ml of methylene chloride and 6.5 ml of water. After stirring at room temperature for 24 hours,Ml of water, washed once with 15 ml of saturated brine, the organic layer was separated, and dried over anhydrous sodium sulfate to remove water After which the solvent was removed on a rotary evaporator and purified using 200-300 mesh silica gel column chromatography (eluent ethyl acetate / petroleum ether volume 1: 30-1: 20) to give 1.41 g of the compound 4 as a colorless solid in a yield of 89%
The synthetic route of 4101-68-2 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Guilin University of Technology; Kong, Xiangfei; Dai, Shengping; Yang, Liu; Liao, Peihai; Wang, Guixia; (8 pag.)CN106117227; (2016); A;,
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bromide – Wiktionary