Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 4263-52-9, name is Sodium 2-bromoethanesulphonate, This compound has unique chemical properties. The synthetic route is as follows., 4263-52-9
A mixture of sodium-2-bromoethanesulfonate (41 1 mg, 1.95 mmol), N-methyltetradecylamine (342 mg, 1.50 mmol), K2C03 (269 mg, 1.95 mmol) and DMF (3 mL) is stirred at 135C bath temperature under argon atmosphere overnight. The volatiies are removed on a rotary evaporator and the residue purified by preparative HPLC to yield 324 mg (64%) of 1 s.1H-NMR (300 MHz, CDCI3): delta = 0.90 (t, J = 6.4, 3H), 1.15-1.45 (m, 22H), 1.78 (m, 2H), 2.97 /2.99 (2s,? = 3H), 3.05-3.55 (m, 5H), 3.64 (m, 1 H), 7.36 (br. s, 1 H).MS (ESI): 336.3 (M+H+), 671.5 (2M+H+), 693.5 (2M+Na+), 709.5 (2M+K+).
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Reference:
Patent; JADO TECHNOLOGIES GMBH; TECHNISCHE UNIVERSITAeT DRESDEN; SCHLECHTINGEN, Georg; KNOeLKER, Hans-Joachim; FRIEDRICHSON, Tim; JENNINGS, Gary; BRAXMEIER, Tobias; WO2012/160187; (2012); A1;,
Bromide – Wikipedia,
bromide – Wiktionary