In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 608-30-0, name is 2,6-Dibromoaniline belongs to bromides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. 608-30-0
[0310] 3 -Chloroperoxy benzoic acid (77%, 11.97 mmol, 2.68 g) was added to a solution of 2,6-dibromoaniline (3.39 mmol; 1.00 g) in chloroform (24 ml). The resulting thick light green suspension was stirred at room temperature overnight. The reaction mixture was diluted with chloroform, washed with saturated aqueous sodium thiosulfate solution (2X), saturated aqueous sodium bicarbonate solution (3X) and brine, dried over anhydrous sodium sulfate and concentrated to afford the titled compound as a light tan solid. This product was taken on to the next step without further purification. NMR (400 MHz, CDCh) delta 7.74 (d, J = 7.96 Hz, 1H), 7.67 (dd, J = 33.6 Hz, J = 8.12 Hz, 1H), 7.25 (m, 1H).
The synthetic route of 608-30-0 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; TEMPLE UNIVERSITY-OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION; CHILDERS, Wayne, E.; ABOU-GHARBIA, Magid, A.; MORTON, George, C.; ISSA, Jean-Pierre, J.; ZHANG, Hanghang; (209 pag.)WO2018/136766; (2018); A1;,
Bromide – Wikipedia,
bromide – Wiktionary