In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 2606-51-1 as follows. 2606-51-1
General procedure: Benzyl bromide (1 g) in dry toluene (15 mL). To this tripheylphosphine (1.5 g) was added and the reaction mixture was refluxed for 1-3 h at 120 C to get the wittig salt as precipitate. It was filtered and washed with dry benzene (yield 62-87%).
According to the analysis of related databases, 2606-51-1, the application of this compound in the production field has become more and more popular.
Reference:
Article; Parihar, Swati; Kumar, Amit; Chaturvedi, Amit K.; Sachan, Naresh Kumar; Luqman, Suaib; Changkija, Bendangla; Manohar, Murli; Prakash, Om; Chanda; Khan, Feroz; Chanotiya; Shanker, Karuna; Dwivedi, Anila; Konwar, Rituraj; Negi, Arvind S.; Journal of Steroid Biochemistry and Molecular Biology; vol. 137; (2013); p. 332 – 344;,
Bromide – Wikipedia,
bromide – Wiktionary